University Sétif 1 FERHAT ABBAS Faculty of Sciences
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Principles of analytical chemistry / VALCARCEL,Miguel
Titre : Principles of analytical chemistry : A textbook Type de document : texte imprimé Auteurs : VALCARCEL,Miguel Editeur : Berlin : Springer Année de publication : 2000 Importance : 1 vol (371 p.) Format : 24 ISBN/ISSN/EAN : 978-3-540-64007-3 Catégories : Chimie Mots-clés : Chimie analytique Index. décimale : 543 Chimie analytique Résumé :
Ce nouveau manuel novateur vise à donner à l'étudiant un avant-goût de ce qu'est essentiellement la chimie analytique, à lui permettre de se faire une idée de cette discipline conforme aux faits actuels et à répondre aux exigences actuelles de l'enseignement scientifique moderne. Les deux textes, chaque chapitre compile des informations sur les objets pédagogiques, sur les contenus, les questions, les séminaires, et une bibliographie annotéeNote de contenu :
Sommaire
Introduction to Analytical Chemistry
1.2 Analytical Chemical Information
1.3 Analytical Chemical References
1.4 Essential Features of Analytical Chemistry
1.4.1 Basic Elements
1.4.2 Fundamentals
1.4.3 Keywords
1.4.4 Developments
1.4.5 Placement
1.4.6 Boundaries
1.5 Evolution of Analytical Chemistry
1.6 Conceptual and Technical Hierarchies
1.7 Classifications
Questions
Seminars
Suggested Readings
Analytical Properties
2.1 Introduction
Uncertainty and Trueness
2.3 Errors in Analytical Chemistry
2.4 Capital Analytical Properties
2.4.1 Accuracy
2.4.2 Representativeness
2.5 Basic Analytical Properties
2.5.1 Precision
2.5.2 Sensitivity
2.5.3 Selectivity
2.6 Accessory Analytical Properties
2.6.1 Expeditiousness
2.6.3 Personnelrelated Factors
2.7.1 Hierarchical Relationships
2.7.2 Foundation Relationships
2.7.4 Complementary Relationships
2.8 Other Analytical Properties
Questions
Numerical Problems
Suggested Readings
Traceability Reference Materials
3.1 Introduction
3.3 Physical and Chemical Traceability
3.4 Types of Standards and their Traceability
3.5 Analytical Chemical Standards
3.5.1 Types
3.5.2 General Properties
3.5.3 Preparation and Storage
3.5.4 Uses
3.5.4.1 Calibration of Equipment and Methods
3.5.4.2 Evaluation of Analytical Processes
3.6 Specific Meanings of Traceability
3.6.2 Traceability of a Sample Aliquot
3.6.3 Traceability of an Instrument
3.6.5 Traceability of a Method
Questions
Seminars
Suggested Readings
The Measurement Process in Chemistry
4.1 Definition of Chemical Measurement Process
4.2 General Steps of a Chemical Measurement Process
4.3 Preliminary Operations
4.3.1 General Features
4.3.2 Substeps
4.3.3 Sampl
4.3.4 Sample Treatment
4.4 Measurement and Transducing of the Analytical Signal
4.5 Signal Acquisition and Data Processing
4.6 Validation of a Chemical Measurement Process
4.7 Salient Current Trends
Annex I
Annex II
Annex III
Annex IV
Annex V
Annex VI
Questions
Seminars
Suggested Readings
Qualitative Aspects of Analytical Chemistry
5.1 Introduction
5.2 The Binary Response
5.2.1 Types of Binary Response
5.2.2 Quantitative Connotations of the Binary Response
5.2.3 Analytical Features of the Binary Response
False Positives and False Negatives
5.3 Types of Qualitative Identification
5.4 Standards and Calibration in Qualitative Analysis
5.5 Classical Qualitative Analysis
5.5.2 Types of Reagents
5.5.3 Analytical Schemes
5.5.3.1 Schemes without Group Separation 222
5.5.3.2 Schemes with Group Separation
5.6 Instrumental Qualitative Analysis
5.6.2 Static Systems
5.6.3 Dynamic Systems
Questions
Seminars
Suggested Readings
Quantitative Aspects of Analytical Chemistry
6.1 Fundamentals
6.1.2 Analytical Properties
6.1.4 Classical and Instrumental Quantitative Analysis
6.1.5 Quantitation Methodologies
6.1.6 Expressing Quantitative Results
6.2 Calculable Quantitation Methods
6.2.1 Absolute Methods Involving no Analytical Standard
6.2.1.1 Gravimetry
6.2.1.2 Coulometry
6.2.2 Absolute Methods Involving Analytical Standards
6.2.2.2 Titrimetry
6.3 Relative Quantitation Methods
6.3.2 Comparative Methods
Questions
Seminars
Suggested Readings
The Analytical Problem
7.2 Meanings of Problem in Analytical Chemistry
7.4 Elements of the Analytical Problem
7.5 Steps of the Analytical Problemsolving Process
7..51 Identifying and Confirming the Information Required
7.5.2 Pinpointing the Analytical Information Required
7.5.3 Planning the Analytical Approach
7.5.4 Monitoring the Results
7.5.5 Implementing Corrective Actions
7.7 The Analytical Problem in the Context of Quality
Questions
Seminars
Analytical Chemistry and Quality
8.1 Introduction
8.2 A Generic Approach to Quality
8.2.2 Types of Quality
8.23 Quality Compromises
824 Structure of Quality
825 Benefits of Quality
8.3 General Aspects of Quality in Analytical Chemistry
8.3.2 Quality and Analytical Properties
8.3.3 Quality and the Analytical Problem
8.4.2 ISO Guide 25 EN45 000
8.4.3 Good Laboratory Practices
8.4.4 Specific Quality Systems Used in Analytical Chemistry
8.5 Analytical Quality Control
8.6 Assessment of Analytical Quality
8.6.2 Laboratory Accreditation
8.6.3 Proficiency Testing
8.7 Supports of Analytical Quality Assurance
8.8 Costs and Benefits of Analytical Quality Systems
Questions
Seminars
Suggested Readings
Glossary of Terms
Symbols and Abbreviations used in the text
Côte titre : Fs/0743-0744 Principles of analytical chemistry : A textbook [texte imprimé] / VALCARCEL,Miguel . - Berlin : Springer, 2000 . - 1 vol (371 p.) ; 24.
ISBN : 978-3-540-64007-3
Catégories : Chimie Mots-clés : Chimie analytique Index. décimale : 543 Chimie analytique Résumé :
Ce nouveau manuel novateur vise à donner à l'étudiant un avant-goût de ce qu'est essentiellement la chimie analytique, à lui permettre de se faire une idée de cette discipline conforme aux faits actuels et à répondre aux exigences actuelles de l'enseignement scientifique moderne. Les deux textes, chaque chapitre compile des informations sur les objets pédagogiques, sur les contenus, les questions, les séminaires, et une bibliographie annotéeNote de contenu :
Sommaire
Introduction to Analytical Chemistry
1.2 Analytical Chemical Information
1.3 Analytical Chemical References
1.4 Essential Features of Analytical Chemistry
1.4.1 Basic Elements
1.4.2 Fundamentals
1.4.3 Keywords
1.4.4 Developments
1.4.5 Placement
1.4.6 Boundaries
1.5 Evolution of Analytical Chemistry
1.6 Conceptual and Technical Hierarchies
1.7 Classifications
Questions
Seminars
Suggested Readings
Analytical Properties
2.1 Introduction
Uncertainty and Trueness
2.3 Errors in Analytical Chemistry
2.4 Capital Analytical Properties
2.4.1 Accuracy
2.4.2 Representativeness
2.5 Basic Analytical Properties
2.5.1 Precision
2.5.2 Sensitivity
2.5.3 Selectivity
2.6 Accessory Analytical Properties
2.6.1 Expeditiousness
2.6.3 Personnelrelated Factors
2.7.1 Hierarchical Relationships
2.7.2 Foundation Relationships
2.7.4 Complementary Relationships
2.8 Other Analytical Properties
Questions
Numerical Problems
Suggested Readings
Traceability Reference Materials
3.1 Introduction
3.3 Physical and Chemical Traceability
3.4 Types of Standards and their Traceability
3.5 Analytical Chemical Standards
3.5.1 Types
3.5.2 General Properties
3.5.3 Preparation and Storage
3.5.4 Uses
3.5.4.1 Calibration of Equipment and Methods
3.5.4.2 Evaluation of Analytical Processes
3.6 Specific Meanings of Traceability
3.6.2 Traceability of a Sample Aliquot
3.6.3 Traceability of an Instrument
3.6.5 Traceability of a Method
Questions
Seminars
Suggested Readings
The Measurement Process in Chemistry
4.1 Definition of Chemical Measurement Process
4.2 General Steps of a Chemical Measurement Process
4.3 Preliminary Operations
4.3.1 General Features
4.3.2 Substeps
4.3.3 Sampl
4.3.4 Sample Treatment
4.4 Measurement and Transducing of the Analytical Signal
4.5 Signal Acquisition and Data Processing
4.6 Validation of a Chemical Measurement Process
4.7 Salient Current Trends
Annex I
Annex II
Annex III
Annex IV
Annex V
Annex VI
Questions
Seminars
Suggested Readings
Qualitative Aspects of Analytical Chemistry
5.1 Introduction
5.2 The Binary Response
5.2.1 Types of Binary Response
5.2.2 Quantitative Connotations of the Binary Response
5.2.3 Analytical Features of the Binary Response
False Positives and False Negatives
5.3 Types of Qualitative Identification
5.4 Standards and Calibration in Qualitative Analysis
5.5 Classical Qualitative Analysis
5.5.2 Types of Reagents
5.5.3 Analytical Schemes
5.5.3.1 Schemes without Group Separation 222
5.5.3.2 Schemes with Group Separation
5.6 Instrumental Qualitative Analysis
5.6.2 Static Systems
5.6.3 Dynamic Systems
Questions
Seminars
Suggested Readings
Quantitative Aspects of Analytical Chemistry
6.1 Fundamentals
6.1.2 Analytical Properties
6.1.4 Classical and Instrumental Quantitative Analysis
6.1.5 Quantitation Methodologies
6.1.6 Expressing Quantitative Results
6.2 Calculable Quantitation Methods
6.2.1 Absolute Methods Involving no Analytical Standard
6.2.1.1 Gravimetry
6.2.1.2 Coulometry
6.2.2 Absolute Methods Involving Analytical Standards
6.2.2.2 Titrimetry
6.3 Relative Quantitation Methods
6.3.2 Comparative Methods
Questions
Seminars
Suggested Readings
The Analytical Problem
7.2 Meanings of Problem in Analytical Chemistry
7.4 Elements of the Analytical Problem
7.5 Steps of the Analytical Problemsolving Process
7..51 Identifying and Confirming the Information Required
7.5.2 Pinpointing the Analytical Information Required
7.5.3 Planning the Analytical Approach
7.5.4 Monitoring the Results
7.5.5 Implementing Corrective Actions
7.7 The Analytical Problem in the Context of Quality
Questions
Seminars
Analytical Chemistry and Quality
8.1 Introduction
8.2 A Generic Approach to Quality
8.2.2 Types of Quality
8.23 Quality Compromises
824 Structure of Quality
825 Benefits of Quality
8.3 General Aspects of Quality in Analytical Chemistry
8.3.2 Quality and Analytical Properties
8.3.3 Quality and the Analytical Problem
8.4.2 ISO Guide 25 EN45 000
8.4.3 Good Laboratory Practices
8.4.4 Specific Quality Systems Used in Analytical Chemistry
8.5 Analytical Quality Control
8.6 Assessment of Analytical Quality
8.6.2 Laboratory Accreditation
8.6.3 Proficiency Testing
8.7 Supports of Analytical Quality Assurance
8.8 Costs and Benefits of Analytical Quality Systems
Questions
Seminars
Suggested Readings
Glossary of Terms
Symbols and Abbreviations used in the text
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