Titre : | Applications of x-ray photoelectron spectroscopy to catalytic studies : from routine analysis to cutting edge surface characterization |
Auteurs : | Spyridon Zafeiratos, Auteur |
Type de document : | document électronique |
Editeur : | New Jersey : World Scientific, 2023 |
Collection : | Catalytic science series, num. 21 |
ISBN/ISSN/EAN : | 978-1-80061-330-0 |
Format : | 1 vol. (548 p.) / ill. |
Langues: | Anglais |
Index. décimale : | 541.395 (Catalyse) |
Catégories : | |
Mots-clés: | Photoelectron Spectroscopy X-ray Photoemission |
Résumé : |
X-ray photoelectron spectroscopy (XPS) has become a standard practice technique, and automated XPS facilities can be found in industry and in universities all over the world. This transformed XPS from an advanced characterization method for dedicated research, to a rather standard analysis technique of surface analysis. The catalyst's surface state is probably the most prominent factor that influences the catalytic performance. It is therefore no surprise that XPS has become an indispensable tool in studies of solid catalysts. It has been directly used to investigate issues such as the surface composition of the active catalyst and reaction and deactivation mechanisms.The objective of this book is to provide a comprehensive overview of the current status and future perspectives of X-ray photoelectron spectroscopy dedicated to catalytic applications, including thermal catalysis, electrocatalysis, and photo(electro)catalysis. The book contains 13 chapters, starting with the necessary introduction of the technique background, including basic phenomena and instrumentation aspects. The second part of the book focuses on the presentation of long-established applications of the technique, such as XPS studies of model catalysts. Finally, the book describes relatively recent developments of this method for cutting-edge surface characterization mainly using synchrotron X-ray radiation. |
Note de contenu : |
Contents: • X-ray Photoelectron Spectroscopy in Catalysis: Impact and Historical Background. • Practical Aspects of XPS: From Sample Preparation to Spectra Interpretation. • Introduction to Chemical State Analysis by XPS with Examples. • The Practical Dos and Don'ts of Using XPS to Qualify and Quantify Powder Catalysts. • XPS Analysis of Electrically Insulating Catalytic Materials. • Assigning XPS Peaks to Chemical Environments Using First-Principles Calculations . • Application of XPS in Studies of Model Catalysts: From Single Crystals to Supported. • Application of Photoelectron Spectroscopy to Align the Energy Levels of Photocatalysts . • Time-Resolved X-ray Photoelectron Spectroscopy for Understanding of the Photocatalytic Phenomenon. • Catalysts at Work by Near-Ambient Pressure X-ray Photoelectron Spectroscopy. • Scanning and Full-Field Imaging Photoelectron Microscopy Studies Relevant to Heterogeneous Catalysis. • Applying XPS to Study Solid/Liquid Interfaces. • NAP-XPS Studies of Mixed Conducting Electrodes During High-Temperature Electrochemical Reactions. |
Côte titre : |
EB/004 |
En ligne : | https://www.worldscientific.com/doi/epdf/10.1142/q0392 |
Exemplaires (1)
Cote | Support | Localisation | Disponibilité |
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EB/004 | Livre | Bibliothèque centrale | Disponible |
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